Analytical Methods in Supramolecular Chemistry (ePub)

Preface Volume One INTRODUCTION Some Historical Remarks on Supramolecular Chemistry The Noncovalent Bond: a Brief Overview Basic Concepts in Supramolecular Chemistry Conclusions: Diverse Methods for a Diverse Research Area QUANTITATIVE ANALYSIS OF BINDING PROPERTIES Theoretical Principles A Practical Course of Binding Constant Determination by UV/Vis Spectroscopy Practical Course of Action for NMR Spectroscopic Binding Constant Determination Other Important Examples with Practical Actions of Data Treatment Conclusion ISOTHERMAL TITRATION CALORIMETRY IN SUPRAMOLECULAR CHEMISTRY Introduction The Thermodynamic Platform Acquiring Experimental Calorimetric Data Extending the Measurement Range Perspectives EXTRACTION METHODS Introduction The Extraction Technique The Technical Process The Extraction Equilibrium Principles of Supramolecular Extraction Examples of Supramolecular Extraction Conclusions and Future Perspectives MASS SPECTROMETRY AND GAS PHASE CHEMISTRY OF SUPRAMOLECULES Introduction Instrumentation Particularities and Limitations of Mass Spectrometry Beyond Analytical Characterization: Tandem MS Experiments for the Examination of the Gas-Phase Chemistry of Supramolecules Selected Examples Conclusions DIFFUSION NMR IN SUPRAMOLECULAR CHEMISTRY AND COMPLEXED SYSTEMS Introduction Concepts of Molecular Diffusion Measuring Diffusion with NMR Applications of Diffusion NMR in Supramolecular Chemistry: Selected Examples Advantages and Limitations of High Resolution Diffusion NMR Diffusion NMR and Chemical Exchange Diffusion Modes and Signal Decay in Diffusion MR Experiments Applications of Diffusion NMR in Complex Systems Summary and Outlook PHOTOPHYSICS AND PHOTOCHEMISTRY OF SUPRAMOLECULAR SYSTEMS Introduction Spectrophotometry and Spectrofluorometry Time-Resolved Fluorescence Techniques Fluorescence Anisotropy Transient Absorption Spectroscopy Concluding Remarks CIRCULAR DICHROISM SPECTROSCOPY Basic Considerations Measurement Techniques (Methodology of CD

Christoph A. Schalley is professor for organic chemistry and modular synthesis at the Free University of Berlin since October 2005. He received his PhD under the supervision of Helmut Schwarz at the Technical University of Berlin followed by a postdoctorate with Julius Rebek, Jr. at The Scripps Research Institute in California. In 1999 he joined the University of Bonn as a Liebig-Fellow of the Fonds der Chemischen Industrie to start his own independent research group. Professor Schalley has authored more than 150 publications and (co-)edited several books on mass spectrometry, dendrimers and template synthesis. He is recipient of Dozentenstipendium of the Fonds der Chemischen Industrie (2004) and the Mattauch-Herzog award of the German Society for Mass Spectrometry (2006). His research interests also include mass spectrometric characterization and gas-phase chemistry of supramolecules.

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